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To get a much better idea of the HPCVD deposition and doping method, we carried out synchrotron micro-X-ray fluorescence (XRF) mapping experiments to quantitatively map the distribution of changeover metal dopants in HPCVD created Fe2+:ZnSe optical fibers. Micro-XRF is a handy method as a result of its large sensitivity and sub-micron spatial resol